Compatibility of self-etching dentin adhesives with resin luting cements

Do-Wan Kim; Sang-Jin Park; Kyoung-Kyu Choi

doi:10.5395/JKACD.2005.30.6.493

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Kim, Park, and Choi: Compatibility of self-etching dentin adhesives with resin luting cements

Original Article

Journal of Korean Academy of Conservative Dentistry

Journal of Korean Academy of Conservative Dentistry 2005; 30(6): 493-504.

Published online: 30 November 2005

DOI: https://doi.org/10.5395/JKACD.2005.30.6.493

Compatibility of self-etching dentin adhesives with resin luting cements

Do-Wan Kim, Sang-Jin Park, Kyoung-Kyu Choi

Department of Conservative Dentistry, Division of Dentistry, Graduate School, Kyung Hee University, Korea.

Corresponding Author: Kyoung-Kyu Choi. Department of Conservative Dentistry, Division of Dentistry, Graduate School, Kyung Hee University, 1, Hoegi Dong, Dongdaemun Gu, Seoul, Korea, 130-702. Tel: 82-2-958-9337, choikkyu@khu.ac.kr

Received 9 August 2005 Revised 6 October 2005 Accepted 20 October 2005

(open-access):

This is an Open Access article distributed under the terms of the Creative Commons Attribution Non-Commercial License (http://creativecommons.org/licenses/by-nc/3.0/) which permits unrestricted non-commercial use, distribution, and reproduction in any medium, provided the original work is properly cited.

Abstract

This study was performed to investigate the compatibility between 4 dentin adhesives and 4 resin luting cements.

Dentin adhesives used in this study were All-Bond 2 (Bisco Inc., Schaumbrug, IL, USA), Clearfil SE-Bond (Kuraray Medical Inc, Osaka, Japan), Prompt L-Pop (3M Dental Products, St. Paul, MN, USA), One-Up Bond F (Tokuyama corp., Tokyo, Japan). Resin luting cements used in this study were Choice (Bisco Inc., Schaumbrug, IL, USA), Panavia F (Kuraray Medical Inc, Osaka, Japan), RelyX ARC (3M Dental Products, St. Paul, MN, USA), Bistite II DC (Tokuyama corp., Tokyo, Japan). Combination of each dentin adhesive and corresponding resin cement was made to 16 experimental groups.

Flat dentin surfaces was created on mid-coronal dentin of extracted mandibular third molars, then dentin surface was polished with 320-grit silicon carbide abrasive papers.

Indirect resin composite block (Tescera, Bisco) was fabricated. Its surface for bonding to tooth was polished with silicon carbide abrasive papers. Each dentin adhesive was treated on tooth surface and resin composite overlay were luted with each resin cement. Each bonded specimen was poured in epoxy resin and sectioned occluso-gingivally into 1.0 mm thick slab, then further sectioned into 1.0 × 1.0 mm² composite-dentin beams. Microtensile bond strength was tested at a crosshead speed of 1.0 mm/min. The data were analysed by one-way ANOVA and Duncan's multiple comparison tests.

The results of this study were as follows;

2-step self-etching dentin adhesive which has additional bonding resin is more compatible than 1-step self-etching dentin adhesive.

Keywords: Compatibility, Self-etching dentin adhesives, Resin luting cements, Microtensile bond strength, Indirect resin composite block, Dentin

Figures and Tables

Figure 1

Schematic representation of micro-tensile bond strength test.

Figure 2

Micro-tensile bond strengths with CH resin cement.

Figure 3

Micro-tensile bond strengths with PA resin cement.

Figure 4

Micro-tensile bond strengths with RE resin cement.

Figure 5

Micro-tensile bond strengths with BI resin cement.

Figure 6

Micro-tensile bond strengths of each dentin adhesive coupled with four resin cements.

Figure 7

SEM photograph of the adhesive interface of CH-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.

Figure 8

SEM photograph of the adhesive interface of BI-AB. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.

Figure 9

SEM photograph of the adhesive interface of PA-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.

Figure 10

SEM photograph of the adhesive interface of RE-SE. Hybrid layer is well formed and resin tags are infiltrated into dentinal tubules deeply.

Figure 11

SEM photograph of the adhesive interface of PA-PL. Hybrid layer is relatively thin, resin tags are rare and short.

Figure 12

SEM photograph of the adhesive interface of RE-PL. Hybrid layer is formed limitedly and resin tags are rare.

Figure 13

SEM photograph of the adhesive interface of CH-OU. Resin tags are poorly formed.

Figure 14

SEM photograph of the adhesive interface of BI-OU. Few resin tags are observed.

Table 1

Dentin adhesives used in this study

Table 2

Resin cements used in this study

Table 3

Experimental Groups

Table 4

Instruction for dentin adhesive systems

Table 5

Instruction for resin cements

Table 6

Micro-tensile bond strength of dentin adhesives with resin luting cements (Mean stength ± SD _MPa)

Groups with the same superscripts are not statistically significant (p = 0.05).

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