Journal List > Korean J Orthod > v.40(3) > 1043625

Jeon, Son, and Kang: Effect of tribochemical silica coating on the shear bond strength of rebonded monocrystalline ceramic brackets

Abstract

Objective

The purpose of this study was to investigate the effect of tribochemical silica coating on the shear bond strength (SBS) of rebonded ceramic brackets using nano-filled flowable composite resin.

Methods

A total of 60 premolars were prepared and divided into 4 equal groups as follows: Tribochemical silica coating (TC) + Transbond XT (XT), TC + Transbond supreme LV (LV), Sandblast treatment (SA) + XT, SA + LV. Treated ceramic brackets were rebonded on the premolars using each adhesive. All samples were tested in shear mode on a universal testing machine.

Results

SBS of silica coated groups were high enough for clinical usage (TCLV: 10.82 ± 1.82 MPa, TCXT: 11.50 ± 1.72 MPa). But, SBS of the sandblast treated groups had significantly lower values than the tribochemical silica coated groups (SALV, 1.23 ± 1.16 MPa; SAXT, 1.76 ± 1.39 MPa; p< 0.05). There was no difference between the shear bond strength by type of adhesive. In the silica coated groups, 77% of the samples showed bonding failure in the adhesive. In the sandblast treated group, all bonding failures occurred at the bracket-adhesive interface.

Conclusions

The result of this study suggest that newly introduced nano-filled flowable composite resin and tribochemical silica coating application on debonded ceramic bracket bases can produce appropriate bond strengths for orthodontic bonding.

Figures and Tables

Fig. 1
SEM photomicrograph of ceramic bracket base (magnification × 30). A, New bracket, silica powders uncoated; B, new bracket, silica powders can be seen; C, silica powders were removed from the bracket base after debonding (modified ARI score 1).
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Fig. 2
Application of shear debonding force.
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Fig. 3
SEM photomicrograph of re-treated ceramic bracket base. A, B, C, Silica coated ceramic bracket. Silica particles can be seen (arrow)(magnification × 30, × 250, × 10,000); D, E, F, sandblasted ceramic bracket (magnification × 30, × 250, × 10,000).
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Fig. 4
Energy dispersive X-ray analysis. A, Silica coated bracket base surface; B, sandblasted bracket base surface.
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Table 1
Comparative mean shear bond strength according to the two surface coating methods and the two types of resin adhesives
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SD, Standard deviation.

Table 2
Two-way analysis of variance (ANOVA) for analysis of reciprocal action between silica coating and adhesive type
kjod-40-184-i002

Df, Degree of freedom.

Table 3
Modified adhesive remnant index scores for the groups tested
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TCLV, Tribochemical silica coating + Transbond Supreme LV; TCXT, tribochemical silica coating + Transbond XT; SALV, sandblast + Transbond Supreme LV; SAXT, sandblast + Transbond XT; BF, bracket fracture; EF, enamel fracture.

Table 4
Comparison of adhesive remnant index scores of rebonded brackets according to silica coating, and adhesive type
kjod-40-184-i004

Same abbreviations as Table 3; -, not applicable.

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