Journal List > J Korean Acad Prosthodont > v.53(4) > 1034841

Yi, Kim, Lee, Han, Yeo, Ha, and Kim: Effect of working time on the film thickness of dental resin cements

Abstract

Purpose

The aim of this study was to compare the film thicknesses of several resin cements as a function of time after mixing and to examine the effect of working time on the film thicknesses.

Materials and methods

The film thickness (㎛) of 4 resin cements (n=10), 1 composite resin (Panavia F 2.0), 3 self-adhesive resin (Clearfil SA luting, Zirconite, RelyX U200) cements was measured at 20-second intervals after mixing of the cements up to 200 seconds under a load of 50 N. Linear regression was fitted to verify the effect of working time on the film thickness of each cement. Data were compared to the working time recommended by manufacturers using Wilcoxon test (α =.05).

Results

All of the materials showed a positive linear correlation between the film thickness and working time. There was no statistically significant difference between the working time based on our results and the values recommended by the manufacturers even though there was a discrepancy between those two values.

Conclusion

The film thickness of resin cements could increase with the increase of working time. Working time to meet the ISO standard of 50-㎛ maximum film thickness could be different from the manufacturer’ s recommended value.

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Fig. 1.
Mean values of the film thicknesses of each cement as a function of time after mixing.
jkap-53-325f1.tif
Table 1.
Resin cements tested in this study
Product Manufacturer Characteristics Mixing method Lot No.
Panavia F2.0 Kurary America, NY, USA Composite resin Proprietary dispenser, A: 00543A
Dual polymerized Hand mixed 20 sec B: 00104A
Clearfil SA luting Kurary America, NY, USA Self-adhesive resin Proprietary dispenser, 0008BA
Dual polymerized Hand mixed 10 sec
Zirconite BJM Lab., Or-Yehuda, Israel Self-adhesive resin Proprietary dispenser, 400050
Dual polymerized Auto mixed
RelyX U200 3M ESPE, MN, USA Self-adhesive resin Proprietary dispenser, 493661
Dual polymerized Hand mixed 10 sec
Table 2.
Manufacturer' s recommended working time and the time when the thickness reached 50 ㎛
Product Recommended working time Mean (SD) Mean Differences P value
Panavia F2.0 3 min. after mixing 140.5 (16.5) -39.5 .109
Clearfil SA Luting 60 sec. after mixing 169.4 (31.1) +109.4 .109
Zirconite 1 - 2 min. 119.9 (3.8) +29.9 .109
RelyX U200 2 min. from start of mixing 75.3 (12.2) -34.7 .109
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