Journal List > J Korean Acad Prosthodont > v.52(4) > 1034798

Goo, Kim, Lee, Han, Yeo, Ha, and Kim: Effect of water storage on the fracture toughness of dental resin cement used for zirconia restoration

Abstract

Purpose

The aim of this study was to compare the fracture toughness of currently available resin cements for zirconia restorations and evaluate the effect of water storage on fracture toughness of those resin cements.

Materials and methods

Single-edge notched specimens (3 mm × 6 mm × 25 mm) were prepared from three currently available dual cure resin cements for zirconia restorations (Panavia F 2.0, Clearfil SA luting and Zirconite). Each resin cement was divided into four groups: immersed in distilled water at 37°C for 1 (Control group), 30, 90, or 180 days (n=5). Specimens were loaded in three point bending at a cross-head speed of 0.1 mm/s. The maximum load at specimen failure was recorded and the fracture toughness (KIC) was calculated. Data were analyzed using one-way ANOVA and multiple comparison Scheffe′ test (α =.05).

Results

In control group, the mean KIC was 3.41 ± 0.64 MN ∙ m−1.5 for Panavia F, 2.0, 3.07 ± 0.41 MN ∙ m−1.5 for Zirconite, 2.58 ± 0.30 MN ∙ m−1.5 for Clearfil SA luting respectively, but statistical analysis revealed no significant difference between them. Although a gradual decrease of KIC in Panavia F 2.0 and gradual increases of KIC in Clearfil SA luting and Zirconite were observed with storage time, there were no significant differences between immersion time for each cement.

Conclusion

The resin cements for zirconia restorations exhibit much higher KIC values than conventional resin cements. The fracture toughness of resin cement for zirconia restoration would not be affected by water storage.(J Korean Acad Prosthodont 2014;52:312-6)

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Table 1.
Experimental materials investigated
Resin cement Lot No. Curing mode Resin matrix Manufacturer
Panavia F2.0 00536A Dual cure MDP Kuraray medical Inc., Okayama, Japan
Clearfil SA luting 00251A Dual cure MDP Kuraray medical Inc., Okayama, Japan
Zirconite 4157 HQBARCZ Dual cure UDMA BJM laboratories Ltd., Or-Yehuda, Israel
TEGDMA
Table 2.
Mean and standard deviation in parenthesis for KIC (MN ∙ m−1.5) of three resin cements at 1 day, 30 days, 90 days and 180 days immersion in distilled water
Material Water storage (day)
1 (Control) 30 90 180
Panavia F 2.0 3.41 (0.64) a,A 3.61 (0.51) A 2.56 (0.19) A 3.19 (0.17) A
Clearfil SA luting 2.58 (0.30) a,B 2.78 (0.20) B 2.53 (0.45) B 2.85 (0.38) B
Zirconite 3.07 (0.41) a,C 3.09 (0.38) C 3.56 (0.70) C 3.79 (0.55) C

Means with the same lower-case letter in each column were not significantly different (P>.05).

Means with the same upper-case letter in each row were not significantly different (P>.05).

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