Journal List > J Korean Acad Prosthodont > v.49(2) > 1034653

Kim, Yeo, Kim, Han, Lee, and Yang: Effect of specimen preparation method on the microtensile bond strength of veneering ceramic to zirconia

Abstract

Purpose

The aim of this study was to investigate effect of specimen preparation method on the microtensile bond strength of veneering ceramic to zirconia core.

Materials and methods

Cylindrical Lava zirconia block (3M ESPE, Seefeld, Germany) was cut into discs using a diamond disc. After sintering, the core specimens were placed in an adjustable mold and veneered with Lava ceram (3M ESPE, Seefeld, Germany). The disc shaped specimen of group 1 was cut into microbars (1×1×7 mm3) using a low speed diamond disc under water cooling (n = 15). The specimen of group 2 was cut into microbars (1.2×1.2×7 mm3) in the same way. Whereafter the microbars were trimmed (1×1×7 mm3) using a thick diamond disc under water cooling (n = 15). The microtensile bond strength was tested in a microtensile tester (Instron 8848, Instron® Co., Norwood, USA). Fractured microtensile specimens were analyzed under a stereomicroscope (MZ6, Leica Microsystems GmbH, Wetzlar, Germany) at magnification ×30.

Results

The microtensile bond strength of group 1 (28.8 ± 7.0 MPa) was significantly higher than group 2 (11.0 ± 3.3 MPa) (P=.00).

Conclusion

It appears advisable to avoid the trimming action, especially high strength ceramic specimens. (J Korean Acad Prosthodont 2011;49:114-9)

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Fig. 1.
Veneered zirconia disc (A) was cut into microbars (B) for conducting microtensile bond strength test.
jkap-49-114f1.tif
Fig. 2.
Microtensile bond strength test. A: microtensile tester, B: before the test, C: after the test.
jkap-49-114f2.tif
Table 1.
Microtensile bond strength value (MPa) of veneering ceramic to zirconia core
  Group 1 Group 2
1 29.8 11.6
2 21.8 10.9
3 29.8 10.4
4 29.1 15.6
5 26.0 19.3
6 33.1 10.7
7 33.0 9.4
8 40.3 6.8
9 20.3 8.4
10 24.3 10.1
11 24.3 7.5
12 21.7 10.0
13 20.1 11.1
14 38.0 14.5
15 40.7 8.0
Mean 28.8 11.0
SD 7.0 3.3
Table 2.
Failure type was classified into two groups: cohesive failure in the Lava ceram and mixed failure
  Group 1 Group 2
Failure type 93% ceramic cohesive 47% ceramic cohesive
  7% mixed 53% mixed

mixed failure: adhesive failure and cohesive failure in the Lava ceram

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